pure99z
Part Number: #10-0165 (208-230V) | #10-0166 (380V)
The pure99-z system is an R&D platform with a high degree of versatility. This highly versatile system enables multiple column packing and up to five fractions with high pressure injection and up to 100mL sample loop. It is the most efficient system for separations and research and development on the market.
pure99x Column Upgrades
pure99 Stand Alone Columns provide separation flexibility that is required for every operation. The high maximum pressure and the variable column length allow optimization of the plate number and retention time. The unit comes as a complete assembly on casters that interfaces with the pure99 to control packed bed compression and provide eluent flow and sample injection.
All columns stand alone, have casters, have dimensions of: 60.96 cm x 60.96 cm x 132 cm, and are manufactured in the USA by United Science
| Max Column Volume | 1.5 L |
| Materials | 316 Stainless Steel, PTFE |
| Inside Diameter | 130 cm |
| Max Pressure | 172 bar |
| Max Column Volume | 1.5 L |
| Materials | 316 Stainless Steel, PTFE |
| Inside Diameter | 140 cm |
| Max Pressure | 344 bar |
| Max Column Volume | 7 L |
| Materials | 316 Stainless Steel, PTFE, Viton |
| Inside Diameter | 178 cm |
| Max Pressure | 195 bar |
| Max Column Volume | 10 L |
| Materials | 316 Stainless Steel, PTFE, Viton |
| Inside Diameter | 178 cm |
| Max Pressure | 195 bar |
| Max Column Volume | 13 L |
| Materials | 316 Stainless Steel, PTFE, Viton |
| Inside Diameter | 203 cm |
| Max Pressure | 284 bar |
pure99z Column Upgrades
pure99 Stand Alone Columns provide separation flexibility that is required for every operation. The high maximum pressure and the variable column length allow optimization of the plate number and retention time. The unit comes as a complete assembly on casters that interfaces with the pure99 to control packed bed compression and provide eluent flow and sample injection.
All columns stand alone and have casters, with the same dimensions of: 60.96 cm x 60.96.cm x 132 cm. Columns are manufactured in the USA by United Science
1.5 L (130 mm)
3 L (140 mm)
7 L (178 mm)
10 L (178 mm)
13 L (203 mm)
| Max Column Volume 1.5 L | Max Column Volume 3 L | Max Column Volume 7 L | Max Column Volume 10 L | Max Column Volume 13 L |
|---|---|---|---|---|
| Materials: 316 Stainless Steel, PTFE | Materials: 316 Stainless Steel, PTFE, Viton | Materials: 316 Stainless Steel, PTFE, Viton | Materials: 316 Stainless Steel, PTFE, Viton | Materials: 316 Stainless Steel, PTFE, Viton |
| Inside Diameter: 130 cm | Inside Diameter: 140 cm | Inside Diameter: 178 cm | Inside Diameter: 178 cm | Inside Diameter: 203 cm |
| Max Pressure: 172 bar | Max Pressure: 344 bar | Max Pressure: 195 bar | Max Pressure: 195 bar | Max Pressure: 284 bar |
pure99z FEATURES & BENEFITS
- High Pressure Column
- Large Diameter Column for High Loadability
- Binary On Line Solvent Gradient Mixing
- Automated Methods & Data Integrity Controls
- Closed Loop Solvent Recycling
PROCESSING POWER:
Sample loop up to 100mL; Pumps able to pressurize up to 5K psi @ 900 mL/min; Column is packable with a variety of materials, selectivity, particle diameter, and pore diameter; High pressure mixing, eliminating need for solvent degassing & helium sparging; State of the art data system to enable automation of methods & data integrity controls
GMP COMPLIANCE:
21 CFR Part 11 compliant software; Material conformity certifications DIN EN 10204 2.2 or FDA 21 CFR 177/178; Inert & chemically stable polymeric seals; UL 698A, Listed; cUL and CSA equivalents; Normal, chiral, and revers phases
PROCESSING CONTROL:
Automated for batch operation; Column, eluent; Temperature control computer; Touchscreen user interface; UV/VIS detectors; Closed loop solvent recovery; Method, sequence, and data acquisition software
General Specifications
| Dimensions (inches) | L104″ x W46″ x H84″ |
| Unit Weight (pounds) | 1800 |
| Sound Pressure (db) | <50 |
CERTIFICATIONS:
UL 698A, Listed; ETL UL 508A Stamped; Wetted Materials FDA approved; ASME 316SS
REQUIRED, SOLD SEPARATELY: Chiller Requirement: 10 tons; Heater Requirement: 48kW, 200 GPM, 460v/3ph/80.6amp
ALSO AVAILABLE, SOLD SEPARATELY:
GMP Documentation Package; Commissioning and Training Package; Maintenance Package (12 Months)
WARRANTY:
12 months for quality, labor, parts, and workmanship on United Science equipment.
The pure99z is designed for research and development operations. Preparative chromatography yields a very high recovery rate compared other competing chromatography techniques. For example, it is not uncommon to recover up to 99% of the target cannabinoid. Liquid-liquid techniques typically have much lower recoveries. High recovery during chromatography depends primarily on the selectivity of separation.
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